Trial Outcomes & Findings for The Effect of Methylphenidate Treatment on Oxidative Stress Levels in Children Diagnosed With Attention Deficit Hyperactivity Disorder (ADHD) (NCT NCT06844812)

NCT ID: NCT06844812

Last Updated: 2025-06-08

Results Overview

Total Oxidant Status (TOS) level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. TOS was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E1599Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Recruitment status

COMPLETED

Target enrollment

39 participants

Primary outcome timeframe

Immediately before starting the treatment and up to the 3rd month of treatment.

Results posted on

2025-06-08

Participant Flow

Initially, 39 patients were enrolled in the study, and each patient who dropped out of the study during follow-up was replaced by a new patient in accordance with the protocol. Thus, a total of 53 patients were included in the study and 14 patients left the study for various reasons.

Participant milestones

Participant milestones
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
Patients diagnosed with attention deficit hyperactivity and planned to start methylphenidate treatment
Overall Study
STARTED
53
Overall Study
COMPLETED
39
Overall Study
NOT COMPLETED
14

Reasons for withdrawal

Reasons for withdrawal
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
Patients diagnosed with attention deficit hyperactivity and planned to start methylphenidate treatment
Overall Study
Lost to Follow-up
5
Overall Study
stigmatization concerns
2
Overall Study
medication refusal
2
Overall Study
concerns about possible side effects
2
Overall Study
wanting to seek another specialist opinion
2
Overall Study
side effects (dizziness)
1

Baseline Characteristics

Race and Ethnicity were not collected from any participant.

Baseline characteristics by cohort

Baseline characteristics by cohort
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Patients diagnosed with attention deficit hyperactivity and planned to start methylphenidate treatment
Age, Continuous
8.38 years
STANDARD_DEVIATION 1.11 • n=39 Participants
Sex: Female, Male
Female
26 Participants
n=39 Participants
Sex: Female, Male
Male
13 Participants
n=39 Participants
Region of Enrollment
Turkey
39 participants
n=39 Participants
Body Weight
27.95 kilogram (kg)
STANDARD_DEVIATION 7.38 • n=39 Participants
body mass index (BMI)
16.60 kilogram(kg)/height(metre)²
STANDARD_DEVIATION 1.96 • n=39 Participants

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Total Oxidant Status (TOS) level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. TOS was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E1599Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Total Oxidant Status
total oxidant status (before starting treatment)
6.29 U/ml
Standard Deviation 5.37
Change in Total Oxidant Status
total oxidant status (after starting treatment)
5.62 U/ml
Standard Deviation 4.76

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Total antioxidant status (TAS) level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment.TAS was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E4350Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Total Antioxidant Status
total antioxidant status (before starting treatment)
7.79 U/ml
Standard Deviation 5.65
Change in Total Antioxidant Status
total antioxidant status (after starting treatment)
7.33 U/ml
Standard Deviation 5.40

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Population: 2 patients were excluded because there was no reaction and no color change in the measurement.

superoxide dismutas level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. Superoxide dismutas was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E0918Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=37 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Superoxide Dismutas
superoxide dismutas (before starting treatment
175.89 U/L
Standard Deviation 158.95
Change in Superoxide Dismutas
superoxide dismutas (after starting treatment)
160.88 U/L
Standard Deviation 143.49

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Malondialdehyde (MDA) level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. MDA was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E1371Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Malondialdehyde
Malondialdehyde (before starting treatment)
9.58 nmol/ml
Interval 7.35 to 9.94
Change in Malondialdehyde
Malondialdehyde (after starting treatment)
8.65 nmol/ml
Interval 7.0 to 13.61

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Ox-LDL level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. Ox-LDL was measured according to the human ELISA kit protocol as follows (bioassay technology laboratory, Cat.No E1521Hu): Standards added to wells. 40μl of serum sample was added to the sample wells, followed by 10μl of anti-TOS antibody. Incubated at 37°C for 60 minutes. plate was washed 5 times with wash buffer. 50μl of substrate solution A was added to the wells and then 50μl of substrate solution B was added to each well. The plate was incubated for 10 minutes at 37°C in the dark. 50μl of Stop Solution was added to the wells and the blue color immediately changed to yellow. The optical density (OD value) of each well was determined using a microplate reader set to 450 nm within 10 min after adding the stop solution.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Ox-LDL
Ox-LDL (before starting treatment)
34.19 ng/mL
Interval 26.36 to 60.96
Change in Ox-LDL
Ox-LDL (after starting treatment)
29.59 ng/mL
Interval 25.24 to 56.67

PRIMARY outcome

Timeframe: Immediately before starting the treatment and up to the 3rd month of treatment.

Oxidative Stress Index (OSI) level was measured according to the human ELISA kit protocol. Serum samples from 39 patients were compared immediately before and after 3 months of treatment. OSI is an index created by the ratio of TOS to TAS. OSI is a parameter that shows the direction in which the body's oxidative stress balance shifts. An increase or decrease in the OSI value indicates that the oxidative balance has changed. While an increase in OSI value indicates a change in balance in favor of oxidants; a decrease in OSI value indicates a change in balance in favor of anti-oxidants.

Outcome measures

Outcome measures
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=39 Participants
Children aged 6 to 11 years with attention deficit hyperactivity
Change in Oxidative Stress Index (OSI)
Oxidative Stress Index (OSI) (before starting treatment)
0.75 Index
Standard Deviation 0.12
Change in Oxidative Stress Index (OSI)
Oxidative Stress Index (OSI) (after starting treatment)
0.72 Index
Standard Deviation 0.12

Adverse Events

Patients Diagnosed With Attention Deficit Hyperactivity

Serious events: 0 serious events
Other events: 26 other events
Deaths: 0 deaths

Serious adverse events

Adverse event data not reported

Other adverse events

Other adverse events
Measure
Patients Diagnosed With Attention Deficit Hyperactivity
n=53 participants at risk
Children aged 6 to 11 years with attention deficit hyperactivity
General disorders
loss of appetite
37.7%
20/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.
General disorders
abdominal pain (temporary)
9.4%
5/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.
General disorders
headache (temporary)
5.7%
3/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.
General disorders
nausea (temporary)
9.4%
5/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.
General disorders
stagnation (temporary)
11.3%
6/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.
General disorders
weight loss
5.7%
3/53 • 3 months
Patients diagnosed with attention deficit hyperactivity and planned to receive methylphenidate treatment were included in the study. Patients eligible for methylphenidate treatment due to indication were included. Therefore, there were no patients at risk of death or serious adverse events.

Additional Information

Dr. Enes Faruk ALTUNKILIÇ

mazhar osman mental and nervous diseases hospital

Phone: +905077362191

Results disclosure agreements

  • Principal investigator is a sponsor employee
  • Publication restrictions are in place